Sep 23 – 27, 2024
Ensenada, México
America/Tijuana timezone

Study of the effect of Nitrogen flow on the structure, chemical composition and plasma generated in the synthesis of TiAlTaNbZrN coatings using the HiPIMS system

Not scheduled
1h 30m
Museo Caracol (Ensenada, México)

Museo Caracol

Ensenada, México

Caracol Centro Científico y Cultural A.C Club Rotario 3, Zona Federal, 22800 Ensenada, B.C.
Poster Plasma and Vacuum PLASMA AND VACUUM

Speaker

Sara Mendoza Castañeda (Departamento Mecánica y Mecatrónica, Universidad Nacional de Colombia)

Description

The aim of research is to evaluate how the nitrogen flow in a HiPIMS system affected plasma and microstructural characterization during the deposition of TiAlTaNbZrN. First, the synthesis conditions for producing the TiAlTaNbZr metallic coatings were optimized by varying the pressure and substrate bias in orden to identify the best conditions in terms of FCC structure (using X-Ray Diffraction (XRD)) and adhesion (using Scratch Test). Subsequently, TiAlTaNbZrN coatings were deposited varying nitrogen flows, and simultaneously the plasma parameters were studied using Optical Emission Spectroscopy (OES). Lastly, the results of plasma characterization were correlated with the microstructure and chemical composition of the films deposited, using XRD for determining crystalline structure and Energy Dispersive Spectroscopy (EDS) for determining the elemental concentration.

Reference

L. Wang, J. Jin, C. Zhu, G. Li, X. Kuang, y K. Huang, “Effects of HiPIMS pulse-length on
plasma discharge and on the properties of WC-DLC coatings”, Appl Surf Sci, vol. 487,
pp. 526–538, sep. 2019, doi: 10.1016/J.APSUSC.2019.05.046.

This work was supported by

Universidad Nacional de Colombia

Keywords Sputtering, HiPIMS, TiAlTaNbZrN, Optical, Plasma
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Author

Sara Mendoza Castañeda (Departamento Mecánica y Mecatrónica, Universidad Nacional de Colombia)

Co-authors

Ms Ingrid Johana González Ávila (Universidad Nacional de Colombia) Dr Jhon Jairo Olaya Florez (Universidad Nacional de Colombia) Mr Juan Pablo González Lozano (Universidad Nacional de Colombia) Dr Óscar Edwin Piamba Tulcán (Universidad Nacional de Colombia)

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